Preparation of Gold Nanoparticles via Anodic Strip** of Copper Underpotential Deposition in Bulk Gold Electrodeposition for High-Performance Electrochemical Sensing of Bisphenol A
Abstract
:1. Introduction
2. Results and Discussion
2.1. Fabrication and Characterization of Modified Electrodes
2.2. Electrocatalysis and Electrochemical Sensing of BPA
2.3. Anti-Interference Capacity and Stability of the AuCu-UPD/MWCNTs/GCE
2.4. Practical Water Sample Analysis
3.3. Electrochemical Measurement of Bisphenol A
4. Conclusions
Supplementary Materials
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Modified Electrode | Detection Method | Sensitivity (μA μM −1) | Linear Range (μM) | LOD (nM) | References |
---|---|---|---|---|---|
CMOF-MIPIL sensor | DPV | 0.1589 | 0.005–5.0 | 4.0 | [32] |
AuNPs-ErCDs-MOFs/GCE | DPV | 6.92 1.84 | 0.07–0.5 0.5–1.3 | 32 | [17] |
WO3-CNT/GCE | DPV | 1.45 0.201 | 0.03–3.0 3.0–100 | 16.3 | [33] |
MWCNTs-βCD/SPCE | LSV | 7.1944 2.159 | 0.125–2.0 2.0–3.0 | 13.7 | [34] |
GO-MWCNT-βCD/SPE | DPV | 10.3 0.85 | 0.03–10 10–120 | 5.0 | [14] |
10%Pt@Ti3C2Tx/GCE | DPV | - | 0.05–5.0 | 32 | [35] |
Hemin/TAPB-DMTP-COF/AuNPs | DPV | 0.013 | 0.01–3.0 | 3.5 | [36] |
AuNPs/mCNTs@ZIF-8 | DPV | 0.99 | 1.0–100 | 690 | [37] |
AuPdNPs/GNs-GCE | DPV | 3.97 | 0.05–10 | 8.0 | [18] |
SWCNT/MCE paper | LSV | - | 0.5–10 25–100 | 82 | [22] |
AuCu-UPD/MWCNTs/GCE | DPV | 21.6 1.68 | 0.01–1 1.0–20 | 2.43 | This work |
Sample | Added (μM) | Found (μM) | Recovery (%) | RSD (%) |
---|---|---|---|---|
0.5 | 0.5205 | 104.1 | 3.2 | |
Tap Water | 2 | 2.054 | 102.7 | 4.1 |
5 | 5.195 | 103.9 | 3.7 | |
0.5 | 0.523 | 104.6 | 2.9 | |
Bottled Water | 2 | 1.83 | 91.5 | 3.6 |
5 | 4.94 | 99.8 | 2.7 | |
0.5 | 0.4888 | 97.76 | 4.5 | |
**angjiang River Water | 2 | 1.961 | 98.05 | 3.9 |
5 | 5.105 | 92.1 | 3.4 |
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Huang, Z.; Chen, Z.; Yan, D.; Jiang, S.; Nie, L.; Tu, X.; Jia, X.; Wågberg, T.; Chao, L. Preparation of Gold Nanoparticles via Anodic Strip** of Copper Underpotential Deposition in Bulk Gold Electrodeposition for High-Performance Electrochemical Sensing of Bisphenol A. Molecules 2023, 28, 8036. https://doi.org/10.3390/molecules28248036
Huang Z, Chen Z, Yan D, Jiang S, Nie L, Tu X, Jia X, Wågberg T, Chao L. Preparation of Gold Nanoparticles via Anodic Strip** of Copper Underpotential Deposition in Bulk Gold Electrodeposition for High-Performance Electrochemical Sensing of Bisphenol A. Molecules. 2023; 28(24):8036. https://doi.org/10.3390/molecules28248036
Chicago/Turabian StyleHuang, Zhao, Zihan Chen, Dexuan Yan, Shuo Jiang, Libo Nie, **nman Tu, Xueen Jia, Thomas Wågberg, and Long Chao. 2023. "Preparation of Gold Nanoparticles via Anodic Strip** of Copper Underpotential Deposition in Bulk Gold Electrodeposition for High-Performance Electrochemical Sensing of Bisphenol A" Molecules 28, no. 24: 8036. https://doi.org/10.3390/molecules28248036